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Coordinators: Pino Verónica, Pasán Jorge, Trujillo Rodríguez Maria José

Language: English

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300 p. · 15x22.8 cm · Paperback

Metal-organic Frameworks in Analytical Sample Preparation and Sensing presents all the areas of applications of metal-organic frameworks in analytical sample preparation. Metal-organic frameworks are crystalline coordination polymers with robust and stable crystal structures, high synthetic tunability, and interesting properties for their use in analytical applications, including their detailed use as sorbents in miniaturized-extraction procedures and as components in sensors. This book also provides important information about the synthesis and characterization of these materials, with useful tips written by experts on the subject with respect to their conditioning, handling, and recycling. Their outstanding properties, adsorptive capabilities, and structural diversity are also highlighted. This will help experts in the field to select the proper metal-organic framework for a particular analytical application.

Section 1: Reticular materials: synthesis, characterization, and properties 1. Introduction and general aspects of metal-organic frameworks and other novel reticular materials 2. Synthesis of metal-organic frameworks with interest in analytical chemistry 3. Synthesis of covalent-organic frameworks with interest in analytical chemistry 4. Synthesis of composites based on reticular materials with interest in analytical chemistry Section 2: Metal-organic frameworks as sorbents in analytical sample preparation 5. Metal-organic frameworks in micro-solid phase extraction 6. Metal-organic frameworks in micro-dispersive solid phase extraction and stir bar sorptive extraction 7. Metal-organic frameworks in magnetic-based methods 8. Metal-organic frameworks in solid-phase microextractionIncludes both in-fiber and in-tube solid-phase microextraction 9. Metal-organic frameworks in thin film microextraction 10. Hyphenating microextraction methods based on metal-organic frameworks with chromatographic techniques Section 3: Metal-organic frameworks as sensors for analysis 11. Metal-organic frameworks as luminescence sensors 12. Metal-organic frameworks as electrochemical sensors 13. Other sensing applications of metal-organic frameworks Section 4: Novel reticular materials in analytical sample preparation and sensing 14. Covalent-organic frameworks in sample preparation 15. Covalent-organic frameworks as sensors for analysis

Dr. Pino is Professor at University of La laguna, and PI of Laboratory of Materials for Chemical Analysis (MAT4LL). She obtained her PhD in Chemistry from Universidad de La Laguna (Spain) in 2002 with Doctorate Extraordinary Award and Special Mention for Young Canary Researchers from the Canary Government. She has conducted several research stays, including Wake Forest University, Canary Institute of Agrarian Research, Iowa State University, The University of Toledo, and University Claude Bernard. She was awarded with a prestigious “Ramón y Cajal” research associate position in 2010 at ULL. She has published over 120 JCR research articles included within JCR, 25 book chapters, an h-index of 39, and over 4800 citations. She has been editor of 5 books of Wiley related to Analytical Separation Science, and has been PI of 5 research consecutive projects with funding of the Spanish Government.
Dr. Pasán is Distinguished Researcher at University of La laguna, and member of Laboratory of Materials for Chemical Analysis (MAT4LL). He obtained his PhD in Physics in 2006, obtaining the Doctorate Extraordinary Award. He has performed research stays in Lawrence Berkeley National Laboratory (USA), European Synchrotron Radiation Facility (France), and Instituto de Ciencia Molecular (Valencia, Spain). She has published more than 150 research publications, and 1 book chapters, with an h-index of 41 and over 4700 citations. He has been participated in more than 10 research projects with funding of the Spanish Government, and he is Academic Editor of Nanomaterials.
Dr. Trujillo-Rodríguez is a Junior Researcher at University of La laguna, and member of Laboratory of Materials for Chemical Analysis (MAT4LL). She obtained her PhD in Chemistry in 2017, obtaining the Doctorate Extraordinary Award. She has worked as researcher in Iowa State University (USA), Universitat de les Illes Balears (Spain), and Consejo Superior de Investigaciones Científicias (CSIC, Spain), and is performing
  • Provides analytical scientists with a unified reference guide for the use of metal-organic frameworks in miniaturized-extraction methods and sensing.
  • Covers aspects related to the development, characterization, conditioning and handling of metal-organic frameworks. Issues of scale-up will be covered too.
  • Addresses the proper metal-organic framework for a particular analytical miniaturized method.